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as a whitish powder, (58% yield) d) Synthse D : acide 3, 5,3 ',5'- ttramthylbiphnyl-4 , 4 ' -dicarboxyliqued) Synthesis D: 3,5,3 ', 5'-tetramethylbiphenyl-4,4'-dicarboxylic acid Le schma ractionnel de cette synthse est reprsent ci dessous :The reaction scheme of this synthesis is represented below: 10,2 g de ttramthylbenzidine (98%, Alfa Aesar) sont mis en suspension dans 39 mL d'acide chlorhydrique concentr (37%, commercialis par la socit Aldrich) 0 0 C