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The sample extracts were analyzed using an ultra-performance liquid chromatography-electrospray ionization-tandem mass spectrometry (UPLC-ESI-MS/MS) system (UPLC, ExionLC AD, MS, Applied Biosystems 6500 Triple Quadrupole, The system was equipped with a UPLC column (Waters Acquity BEH C18, 1.7 m, 2.1 mm 100 mm)

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